Dr. Rogers's Publication List: 1989-1990

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(135) "The photoinduced reaction of the tricarbonyl hydride complex Cp'W(CO)₃H (Cp' = η⁵-C₅H₅, η⁵-C₅Me₅) with methylacetylene and dimethylacetylene to give η³-allyl- and metallacyclic alkenyl ketone complexes. Molecular structure of C₅Me₅W(CO)₂ (η³-C₃H₅)." Alt, H. G.; Engelhardt, H. E.; Wrackmeyer, B.; Rogers, R. D., J. Organomet. Chem. 379, 289-301 (1989).

(136) "Photoinduced reactions of the complexes (η⁶-C₆H₃R₃)(CO)₃Cr (R = Me, Et) with the acetylenes R'CCR' (R' = H, C₃H₇, C(OEt)₂H). The molecular structure of (C₆H₃Me₃)(CO)Cr(μ-CO){μ-C₂[C(OEt)₂H]₂}Cr(CO)₄." Alt, H. G.; Engelhardt, H. E.; Rogers, R. D.; Abu-Orabi, S. T., J. Organomet. Chem. 378, 33-43 (1989).

(137) "Preparation and characterization of isonitrile-hydrido complexes Cp'(CO)₂(CNR)MH (Cp' = η⁵-C₅H₅, η⁵-C₅Me₅; R = Me, CMe₃; M = molybdenum, tungsten). Molecular structure of C₅Me₅(CO)₂(CNCMe₃)MoH." Alt, H. G.; Engelhardt, H. E.; Frister, T.; Rogers, R. D., J. Organomet. Chem. 366, 297-304 (1989).

(138) "Reactions of asymmetric binuclear dioxotungsten complex C₅Me₅(CO)₃WW(O)₂C₅Me₅ with chlorine, bromine, iodine, hydrogen chloride, trifluoroacetic acid, nitrosyl chloride, nitrogen monoxide and air. Molecular structure of C₅Me₅W(CO)₂Br₃." Alt, H. G.; Engelhardt, H. E.; Hayen, H. I.; Rogers, R. D., J. Organomet. Chem. 366, 287-95 (1989).

(139) "Protonation of ylide complexes of manganese with tetrafluoroboric acid (HBF₄). Molecular structure of [C₅H₅(CO)₂MnCH₂CH(PEt₃)]BF₄." Alt, H. G.; Engelhardt, H. E.; Rogers, R. D., J. Organomet. Chem. 362, 117-24 (1989).

(140) "Indium(III) compounds containing the neopentyl substituent, In(CH₂CMe₃)₃, In(CH₂CMe₃)₂Cl, In(CH₂CMe₃)Cl₂, and In(CH₂CMe₃)₂CH₃. Crystal and molecular structure of dichloroneopentyl indium(III), an inorganic polymer." Beachley, O. T., Jr.; Spiegel, E. F.; Kopasz, J. P.; Rogers, R. D., Organometallics 8, 1915-21 (1989).

(141) "Preparation, crystal structures, and spectroscopic characterization of diaminochalcogenophosphonium cations." Burford, N.; Spence, R. E. v. H.; Rogers, R. D., J. Am. Chem. Soc. 111, 5006-8 (1989).

(142) "Structure of all-trans-1,6-diphenyl- (A) and all-trans-1,6-bis(o-methoxyphenyl)-1,3,5-hexatriene (B)." Hall, T.; Bachrach, S. M.; Spangler, C. W.; Sapochak, L. S.; Lin, C. T.; Guan, H. W.; Rogers, R. D., Acta Cryst., Sect. C C45, 1541-3 (1989).

(143) "The crystal structure of aquabis(acetonitrile)dichlorodioxouranium bis(acetonitrile) solvate." Hall, T. J.; Mertz, C. J.; Bachrach, S. M.; Hipple, W. G.; Rogers, R. D., J. Cryst. Spectroscop. Res. 19, 499-505 (1989).

(144) "Novel monopentamethylcyclopentadienyl alkoxides of lanthanum and cerium; x-ray crystal structure of [C₅Me₅Ce(OCMe₃)₂]₂." Heeres, H. J.; Teuben, J. H.; Rogers, R. D., J. Organomet. Chem. 364, 87-96 (1989).

(145) "Mono(pentamethylcyclopentadienyl) complexes of cerium(III). Synthesis, molecular structure, thermal stability, and reactivity of (C₅Me₅)CeX₂ (X = 2,6-di-tert-butylphenoxo, CH(SiMe₃)₂, and N(SiMe₃)₂) complexes." Heeres, H. J.; Meetsma, A.; Teuben, J. H.; Rogers, R. D., Organometallics 8, 2637-46 (1989).

(146) "Crystal structures and solution electronic absorption and MCD spectra for perchlorate and halide salts of binuclear gold(I) complexes containing bridging Me₂PCH₂PMe₂ (dmpm) or Me₂PCH₂CH₂PMe₂ (dmpe) ligands." Jaw, H. R. C.; Savas, M. M.; Rogers, R. D.; Mason, W. R., Inorg. Chem. 28, 1028-37 (1989).

(147) "Synthesis of [η⁵-(diphenylphosphino)cyclopentadienyl][η⁷-(diphenylphosphino)cycloheptatrienyl]titanium and its utility in the formation of heterobimetallic complexes: the molecular structure of tetracarbonyl{[η⁵-(diphenylphosphino)cyclopentadienyl][η⁷-(diphenylphosphino)cycloheptatrienyl]titanium-P,P'}chromium hemitoluene solvate." Kool, L. B.; Ogasa, M.; Rausch, M. D.; Rogers, R. D., Organometallics 8, 1785-90 (1989).

(148) "A new system of ionophors derived from o,o'-biphenyldiol. X-ray structure of o-hydroxy-biphenyl-o'-oxyacetamide." Lin, W. O.; Da Costa, J. B. N.; Alt, H. G.; Rogers, R. D., Z. Naturforsch., B: Chem. Sci. 44, 1331-2 (1989).

(149) "Synthesis of [alkenyl(dimethylamino)carbene]tungsten complexes using the Peterson reaction. X-ray crystal structure of E-(CO)₅W[C(NMe₂)CH:CH(η-C₅H₄)Fe(η-C₅H₅)]." Macomber, D. W.; Madhukar, P.; Rogers, R. D., Organometallics 8, 1275-82 (1989).

(150) "Stereoselective formation from a (1S,5S)-(-)-verbenone-derived cyclopentadiene of dimeric and mixed titanium and zirconium dichloride complexes." Moriarty, K. J.; Rogers, R. D.; Paquette, L. A., Organometallics 8, 1512-17 (1989).

(151) "Isodicyclopentadienes and related molecules. Part 41. Stereochemical course of Diels-Alder cycloadditions to (hydroxymethyl)-substituted plane-nonsymmetric cyclopentadienes." Paquette, L. A.; Vanucci, C.; Rogers, R. D., J. Am. Chem. Soc. 111, 5792-800 (1989).

(152) "Isodicyclopentadienes and related molecules. 48. Stereochemically uniform mode of iron carbonyl complexation to spirocyclic isodicyclopentadienes." Paquette, L. A.; O'Doherty, G. A.; Miller, B. L.; Rogers, R. D.; Rheingold, A. L.; Geib, S. L., Organometallics 8, 2167-72 (1989).

(153) "Isodicyclopentadienes and related molecules. 43. Stereochemical course of p-face coordination to isodicyclopentadiene during formation of mixed titanocene and zirconocene dichloride complexes." Paquette, L. A.; Moriarty, K. J.; Meunier, P.; Gautheron, B.; Sornay, C.; Rogers, R. D.; Rheingold, A. L., Organometallics 8, 2159-67 (1989).

(154) "Isodicyclopentadienes and related molecules. 44. Analysis of the π-facial preference for complexation of a camphor-derived, enantiomerically pure cyclopentadienyl ligand to CpMCl₂ fragments (M = Ti and Zr)." Paquette, L. A.; Moriarty, K. J.; McKinney, J. A.; Rogers, R. D., Organometallics 8, 1707-13 (1989).

(155) "Isodicyclopentadienes and related molecules. 45. (1R)-(-)-Nopol as the source of an optically pure fused cyclopentadienyl ligand. Stereochemical course of complexation to cyclopentadienyltitanium and -zirconium dichloride fragments." Paquette, L. A.; Moriarty, K. J.; Rogers, R. D., Organometallics 8, 1506-11 (1989).

(156) "Comparative analysis of molecular-recognition levels attained during capture of chiral cyclopentenyl organometallics by conformationally immobilized ketonic systems." Paquette, L. A.; He, W.; Rogers, R. D., J. Org. Chem. 54, 2291-300 (1989).

(157) "Anticancer agent development: x-ray crystal structure and keto-enol tautomerism of dimethyl 1-hydroxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl-trans-3,4-dihydronaphthalene-2,3-dicarboxylate." Peterson, J. R.; Winter, T. J.; Do, H. D.; Rogers, R. D., J. Cryst. Spectroscop. Res. 19, 135-45 (1989).

(158) "Anticancer agent development. 3. X-ray structure of dimethyl 1-methoxy-6,7-methylenedioxy-4-(3,4,5-trimethoxyphenyl)-trans-3,4-dihydronaphthalene-2,3-dicarboxylate." Peterson, J. R.; Do, H. D.; Rogers, R. D., Acta Cryst., Sect. C C45, 1568-71 (1989).

(159) "Platelet activating factor antagonist design. 3. X-ray crystal structure and intermolecular crystal lattice interactions of methyl trans-4-acetoxymethyl-4,5-dihydro-2,5-bis(3,4-methylenedioxyphenyl)-3-furancarboxylate." Peterson, J. R.; Horsley, D. B.; Brozik, J. A.; Rogers, R. D., Acta Cryst., Sect. C C45, 1164-7 (1989).

(160) "Platelet activating factor antagonist design. 2. X-ray structure of dimethyl 2,3,4,5-tetrahydro-5b-(3,4-methylenedioxyphenyl)-2-oxo-3β-(3,4,5-trimethoxybenzoyl)-3α,4α-furandicarboxylate." Peterson, J. R.; Do, H. D.; Rogers, R. D., Acta Cryst., Sect. C C45, 1059-63 (1989).

(161) "Platelet activating factor antagonist design: structure of methyl trans-5-(3,4-dimethoxyphenyl)-2,3,4,5-tetrahydro-2-oxo-4-furancarboxylate." Peterson, J. R.; Smillie, T. J.; Rogers, R. D., Acta Cryst., Sect. C C45, 297-300 (1989).

(162) "Novel manganese(III) oxidation chemistry: x-ray crystal structure of 5,7,8-trimethoxy-1-(2,4,5-trimethoxyphenyl)-1,2-dihydronaphthalene." Peterson, J. R.; Winter, T. J.; Everson, T. P.; Rogers, R. D., Acta Cryst., Sect. C C45, 132-4 (1989).

(163) "Synthetic and x-ray structural studies on pentabenzylcyclopentadienyl derivatives of manganese, rhenium, and iron." Rausch, M. D.; Tsai, W. M.; Chambers, J. W.; Rogers, R. D.; Alt, H. G., Organometallics 8, 816-21 (1989).

(164) "Unexpected conformation of the hydrogen chloride salt of [14]aneN4: an x-ray structural examination of [H₂[14]aneN₄H₂]Cl₄ and its role in organoaluminum host-guest chemistry." Robinson, G. H.; Sangokoya, S. A.; Pennington, W. T.; Self, M. F.; Rogers, R. D., J. Coord. Chem. 19, 287-94 (1989).

(165) "Macrocycle complexation chemistry. 31. The crystal structure of heptaaquadichlorothorium(2+) dichloride.18-crown-6 dihydrate." Rogers, R. D., Lanth. Act. Res. 3, 71-81 (1989).

(166) "f-Element/crown ether complexes. Part 28. Novel unidentate coordination of a crown ether and of a polyethylene glycol to uranium(VI)." Rogers, R. D.; Benning, M. M.; Etzenhouser, R. D.; Rollins, A. N., J. Chem. Soc., Chem. Commun., 1586-8 (1989).

(167) "Reactions of acetylenechromium complex (C₆H₃Me₃)(CO)₂Cr(C₂H₂) with trimethylphosphine and dimethylamine. Solid state structure of (C₆H₃Me₃)(CO)₂Cr(PMe₃) and (C₆H₃Me₃)(CO)₂Cr[C(Me)NMe₂]." Rogers, R. D.; Alt, H. G.; Engelhardt, H. E., J. Organomet. Chem. 366, 305-12 (1989).

(168) "f-Element/crown ether complexes. 21. Conformational changes in metal complexed versus hydrogen bonded benzo-15-crown-5 in the structure of [Y(OH₂)₃(NCMe)-(benzo-15-crown-5)][ClO₄]₃·benzo-15-crown-5·CH₃CN." Rogers, R. D., J. Inclusion Phenom. Mol. Rec. Chem. 7, 277-87 (1989).

(169) "Structure of (η⁵-C₅Me₅)(η⁸-C₈H₈)Zr, an aromatic mixed sandwich complex of zirconium(III)." Rogers, R. D.; Teuben, J. H., J. Organomet. Chem. 359, 41-7 (1989).

(170) "Structure of crystal violet tetraphenylborate." Spangler, B. D.; Vanysek, P.; Hernandez, I. C.; Rogers, R. D., J. Cryst. Spectroscop. Res. 19, 589-96 (1989).

(171) "Reaction of 1,2-di-3-indenylethane dianions with photochemically activated carbonyl complexes of chromium, molybdenum and tungsten. Molecular structure of C₉H₇CH₂CH₂C₉H₇ and (η⁵:η⁵-C₉H₆CH₂CH₂C₉H₆)[W(CO)₃Me]₂." Alt, H. G.; Palackal, S. J.; Rogers, R. D., J. Organomet. Chem. 388, 105-16 (1990).

(172) "The chemistry of diphenylphosphine adducts of tris(neopentyl) and tris(trimethylsilylmethyl)gallium and -indium including the crystal and molecular structure of (Me₃CCH₂)₃Ga·P(H)Ph₂." Banks, M. A.; Beachley, O. T., Jr.; Maloney, J. D.; Rogers, R. D., Polyhedron 9, 335-42 (1990).

(173) "Chemistry of the diaminochalcogenophosphinic chloride-aluminum trichloride system: preparation and crystal structures of new chalcogenophosphonium cations." Burford, N.; Spence, R. E. H.; Rogers, R. D., J. Chem. Soc., Dalton Trans., 3611-19 (1990).

(174) "Coordinatively unsaturated Group 15 elements: the isolation and crystal structure of a novel dimeric dithiarsolidinium cation." Burford, N.; Royan, B. W.; Whalen, J. M.; Richardson, J. F.; Rogers, R. D., J. Chem. Soc., Chem. Commun., 1273-5 (1990).

(175) "Syntheses and crystal structures for the first two examples of the four-membered PNSiS heterocycle." Burford, N.; Spence, R. E. H.; Whalen, J. M.; Rogers, R. D.; Richardson, J. F., Organometallics 9, 2854-6 (1990).

(176) "Nuclear magnetic resonance spectroscopic characterization and the crystal and molecular structures of triphenylphosphine sulfide-aluminum trichloride (1/1) and triphenylphosphine selenide-aluminum trichloride (1/1): a classification of the coordinative bonding modes of the phosphine chalcogenides." Burford, N.; Royan, B. W.; Spence, R. E. v. H.; Rogers, R. D., J. Chem. Soc., Dalton Trans., 2111-17 (1990).

(177) "Linear coordinative bonding at oxygen: a spectroscopic and structural study of phosphine oxide-Group 13 Lewis acid adducts." Burford, N.; Royan, B. W.; Spence, R. E. v. H.; Cameron, T. S.; Linden, A.; Rogers, R. D., J. Chem. Soc., Dalton Trans., 1521-8 (1990).

(178) "Organogallium chemistry of macrocyclic amines. Synthesis and molecular structure of [Ga(CH₃)₃]₄[(CH₃)₄[14]aneN₄] and [Ga(CH₃)]₂[14]aneN₄[Ga(CH₃)₃]₂." Lee, B.; Pennington, W. T.; Robinson, G. H.; Rogers, R. D., J. Organomet. Chem. 396, 269-78 (1990).

(179) "Thermal reactions of acyloxy and alkoxy carbene complexes with imines: metathesis, acetate rearrangements, and a new route to imino carbene complexes via Peterson type eliminations." Murray, C. K.; Warner, B. P.; Dragisich, V.; Wulff, W. D.; Rogers, R. D., Organometallics 9, 3142-51 (1990).

(180) "Comparative analysis of diastereoselection levels attainable during controlled exo and endo addition of chiral cyclopentenyl organometallics to optically pure and racemic 1-vinyl-2-norbornanones." Paquette, L. A.; DeRussy, D. T.; Vandenheste, T.; Rogers, R. D., J. Am. Chem. Soc. 112, 5562-73 (1990).

(181) "[4.4.4]Propellahexaene by triple Shapiro degradation. Structural and electronic properties of this maximally unsaturated hydrocarbon and consequences of O-methylation of its [4.4.4]propellatrienetrione precursors." Paquette, L. A.; Liang, S.; Waykole, L.; DeLucca, G.; Jendralla, H.; Rogers, R. D.; Kratz, D.; Gleiter, R., J. Org. Chem. 55, 1598-611 (1990).

(182) "[3.3] Sigmatropy within 1-vinyl-2-alkenyl-7,7-dimethyl-exo-norbornan-2-ols. The first atropselective oxyanionic Cope rearrangement." Paquette, L. A.; Pegg, N. A.; Toops, D.; Maynard, G. D.; Rogers, R. D., J. Am. Chem. Soc. 112, 277-83 (1990).

(183) "Boat/chair topographic stereoselection during anionic oxy-Cope rearrangement of 1-alkenyl-2-cyclopentenyl-endo-norbornan-2-ols." Paquette, L. A.; Teleha, C. A.; Taylor, R. T.; Maynard, G. D.; Rogers, R. D.; Gallucci, J. C.; Springer, J. P., J. Am. Chem. Soc. 112, 265-77 (1990).

(184) "Quantitation of proximity effects on rate. A case study involving dyotropic hydrogen migration within syn-sesquinorbornene disulfones carrying central substituents having different spatial demands." Paquette, L. A.; Kesselmayer, M. A.; Rogers, R. D., J. Am. Chem. Soc. 112, 284-91 (1990).

(185) "Anticancer agent development. 5. X-ray structure and proton MNR spectral analysis of (1α,2α,5α,6α)-2,6-bis(3,4-methylenedioxyphenyl)-3,7-dioxabicyclo[3.3.0]octane-4,8-dione." Peterson, J. R.; Peterson, S.; Baker, J. K.; Rogers, R. D., J. Cryst. Spectroscop. Res. 20, 327-33 (1990).

(186) "Platelet-activating-factor antagonist design. 4. Structure and intermolecular crystal lattice interactions of cis-3,4-dibenzyl-2-oxo-2,3,4,5-tetrahydrofuran." Peterson, J. R.; Horsley, D. B.; Rogers, R. D., Acta Cryst., Sect. C C46, 872-5 (1990).

(187) "Novel manganese(III) oxidation chemistry: x-ray crystal structures of (1α,2α,4β)-1,2-diacetoxy-4-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene (compound A) and (1α,2α,4β)-1,2-diacetoxy-4-(2-methoxyphenyl)-8-methoxy-1,2,3,4-tetrahydronaphthalene (compound B)." Peterson, J. R.; Everson, T. P.; Rogers, R. D., J. Cryst. Spectroscop. Res. 20, 37-45 (1990).

(188) "Anticancer agent development. 4. X-ray crystal structure and intermolecular crystal lattice interactions of methyl trans-4,5-dihydro-4-acetoxymethyl-5-(3,4,5-trimethoxyphenyl)-2-(3,4-methylenedioxyphenyl)-3-furancarboxylate." Peterson, J. R.; Horsley, D. B.; Brozik, J. A.; Rogers, R. D., J. Cryst. Spectroscop. Res. 20, 47-52 (1990).

(189) "Synthetic and structural studies on (η⁵:η⁵-fulvalene)bimetallic compounds derived from (η⁵:η⁵-fulvalene)dithallium." Rausch, M. D.; Spink, W. C.; Conway, B. G.; Rogers, R. D.; Atwood, J. L., J. Organomet. Chem. 383, 227-52 (1990).

(190) "f-Element/crown ether complexes. 20. Synthesis and structure of [Y(NO₃)₃(OH₂)₃]·1.5(15-crown-5)·Me₂CO." Rogers, R. D.; Royal, J. D.; Bolton, D. M.; Boeyens, J. C. A.; Allen, C. C., J. Cryst. Spectroscop. Res. 20, 525-33 (1990).

(191) "Macrocycle complexation chemistry. 33. Preparation of [Ca(12-crown-4)₂][UO₂Cl₄] and [Ca(OH₂)₃(15-crown-5)] [UO₂Cl₄]: structure of [Ca(OH₂)₃(15-crown-5)][UO₂Cl₄]." Rogers, R. D.; Bond, A. H.; Hipple, W. G., J. Cryst. Spectroscop. Res. 20, 611-16 (1990).

(192) "Crystal structures of (η⁵-C₅H₄COMe)M(CO)₃Me (M = Mo, W)." Rogers, R. D.; Atwood, J. L.; Rausch, M. D.; Macomber, D. W., J. Cryst. Spectroscop. Res. 20, 555-60 (1990).

(193) "Structure of 3-(4-methoxyphenyl)-4-phenyl-4H-1,2,4-triazole." Rogers, R. D.; Park, M. G.; Kevill, D. N., Acta Cryst., Sect. C C46, 2218-21 (1990).

(194) "Macrocycle complexation chemistry. 30. Comparison of the crystal structures of [La(NO₃)₃(15-crown-5)] and [La(NO₃)₃(monoaza-15-crown-5)]." Rogers, R. D.; Rollins, A. N., J. Cryst. Spectroscop. Res. 20, 389-93 (1990).

(195) "Macrocycle complexation chemistry. 32. Modification of the lanthanide ion coordination sphere via electrocrystallization of hydrated lanthanide chloride complexes of 12-crown-4." Rogers, R. D.; Nunez, L., Inorg. Chim. Acta 172, 173-80 (1990).

(196) "f-Element/crown ether complexes. 27. The synthesis and crystal structure of [Ce(NO₃)₃(OH₂)(12-crown-4)]·12-crown-4." Rogers, R. D.; Rollins, A. N.; Etzenhouser, R. D.; Henry, R. F., J. Inclusion Phenom. Mol. Rec. Chem. 8, 375-82 (1990).

(197) "Macrocycle complexation chemistry. 29. Synthesis and crystal structure of chloro(18-thiacrown-6)copper polymer." Rogers, R. D.; Nunez, L., J. Coord. Chem. 21, 111-18 (1990).

(198) "Molecular structure of ylidic carbene complex (C₅H₄Me)(CO)₂Mn[CHCH(PEt₃)]." Rogers, R. D.; Alt, H. G.; Maisel, H. E., J. Organomet. Chem. 381, 233-8 (1990).

(199) "Lanthanides and actinides; annual survey covering the year 1983." Rogers, R. D.; Rogers, L. M., J. Organomet. Chem. 380, 51-76 (1990).

(200) "Isodicyclopentadienes and related molecules. LII. Comparative analysis of the solid state structural features of bis[η⁵-(1R,8R)]- and [η⁵-(1R,8R),η⁵-(1S,8S)-7,7,9,9-tetramethyltricyclo[6.1.1.02,6]deca-3,5-dien-2-yl]dichlorotitanium." Sivik, M. R.; Rogers, R. D.; Paquette, L. A., J. Organomet. Chem. 397, 177-85 (1990).

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