Chem 237
Spring 2006

|
Class Schedule
Spring 2006
| Week of |
Experiment |
Reading Assignment |
| Jan 23rd |
Check-in |
Introduction
Appendices I-VI |
| Jan 30th |
Safety Quiz
Experiment 1 (50 points)
Separation of the components of "Panacetin" |
Safety Section of Introduction
Experiments 2-3
Oper: 4,6, 11-13, 14, 21, 23, 28 |
| Feb 6th |
Complete Experiment 1
Experiment 2 (50 points)
Stereochemistry of the addition of bromine to trans-cinnamic
acid |
Experiment 23
Oper: 9, 10, 12, 21, 28 |
| Feb 13th |
Experiment 3 (50 points)
Synthesis of Banana Oil
Experiment 1 report due |
Experiment 5
Oper: 19, 20, 25, 32 |
| Feb 20th |
Complete Experiment 3
Experiment 4 (50 points)
Dehydration of methylcyclohexanols
Experiment 2 report due |
Experiment 21
Oper: 19, 20, 25, 32, 35 |
| Feb 27th |
Experiment 5 (50 points)
TLC analysis of drug mixtures
Experiment 3 report due |
Experiment 15
Oper: 11, 17 |
| March 6th |
Experiment 6 (100 points)
Synthesis of triphenylmethanol and the trityl cation
Experiment 4 report due |
Experiment 31
Oper: 6, 9-14, 19-23, 28, 34, 35 |
| March 13th |
Complete Experiment 6
Synthesis of the trityl cation
Experiment 5 report due |
Experiment 31
Oper: 6, 9-14, 19-23, 28, 34, 35 |
| March 20th |
Spring Break |
|
| March 27th |
Class will meet on 3/27, but
only Friday lab will meet this week
Experiment 7 (100 points)
Friedel-Crafts acylation of anisole |
Experiment 37
Oper: 6, 9, 10, 12, 19, 21, 22, 25, 28, 34, 35 |
| April 3rd |
Experiment 7 (100 points)
Friedel-Crafts acylation of anisole Experiment 6 report
due
Due to Honors Week, the Friday lab will begin Exp 7 on 3/31. |
Experiment 37
Oper: 6, 9, 10, 12, 19, 21, 22, 25, 28, 34, 35 |
| April 10th |
Complete Experiment 7 |
|
| April 17th |
Experiment 8 (100 points)
Aldol condensation of an unknown aldehyde and an unknown ketone
Experiment 7 report due |
Handout
Oper: 12-14, 23, 28, 34, 35
|
| April 24th |
Complete Experiment 8
NMR and IR analysis of product
Experiment 9 (50 points)
Spectroscopic identification of an unknown (Take home) |
Handout
Oper: 34 and 35 |
| May 1st |
Examination
Experiments 8 and 9 reports due
Check out (failure to check out will result in
a charge to your student account) |
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